HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 19738537, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 3-Chloro-1-butene | HCID 11242 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Ethyl 2,2-dimethoxyethylcarbamate | HCID 10921057 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 19738537 | HCID 19738537 | — |
Reaction Steps
22 g (0.24 mol) of 3-chloro-1-butene are added to 35.5 g (0.2 mol) of ethyl N-(2,2-dimethoxyethyl)-carbamate and 26 g of powdered potassium hydroxide in 400 ml of dimethylformamide and the mixture is warmed overnight to 40° C. The salts are dissolved with water and the mixture is extracted several times with methylene chloride. The organic extracts are dried over potassium carbonate and concentrated, and the residue is distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05177210 |
| Source dataset | uspto-grants-1993_01 |
| ORD ID | ord-73c831a286ef4e12b6e586ef2141c8bd |
| Source note | uspto-grants-1993_01 |