HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19100964, compound → HCID 16228902, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19100964 | HCID 19100964 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 16228902 | HCID 16228902 | — |
Reaction Steps
96.5 g (0.279 mol) of diethyl 2-benzyl-2,7-diazabicyclo[3.3.0]octane-3,7-dicarboxylate in 1 l of ethanol are hydrogenated at 100° C. and 100 bar on 5 g of palladium-active carbon (10% Pd). The catalyst is filtered off with suction, the filtrate is concentrated and the residue is distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05177210 |
| Source dataset | uspto-grants-1993_01 |
| ORD ID | ord-b96b4ffeffe243fcbe27e5972620a7df |
| Source note | uspto-grants-1993_01 |