HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → HCID 23678949, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | 2-[(4,6-Dimethoxypyrimidin-2-yl)oxy]-3-ethoxy-3-methylbutanoic acid | HCID 15767152 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 23678949 | HCID 23678949 | 99.3% |
Reaction Steps
To Compound 52 (30.0 g, 0.1 mol) prepared in the above (2) dissolved in methanol (100 ml) was added sodium methoxide (19.3 g, 28% methanol solution), and the mixture was stirred for 10 minutes. Subsequently, methanol was removed under reduced pressure to obtain 32 g of the title compound as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05178663 |
| Source dataset | uspto-grants-1993_01 |
| ORD ID | ord-0f35a6820bf24157b3cc4cc1e8caa4e4 |
| Source note | uspto-grants-1993_01 |