Benzaldehyde → HCID 54080145, compound

HRID 1646167Notes

Reaction equation

HRID 1646167 reaction equation
[CH3:1][N:2]1[C:7]2[CH:8]=[CH:9][C:10]([C:12](=[O:14])[CH3:13])=[CH:11][C:6]=2[S:5][CH2:4][C:3]1=[O:15].C(=O)CC.[CH:20](=O)[C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1>>[CH3:1][N:2]1[C:7]2[CH:8]=[CH:9][C:10]([C:12](=[O:14])[CH:13]=[CH:20][C:21]3[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=3)=[CH:11][C:6]=2[S:5][CH2:4][C:3]1=[O:15]

Participants

4

Reactant 3

HCID 240BenzaldehydeHCID 527PropanalHCID 19801712HCID 19801712, compound

Product 1

HCID 54080145HCID 54080145, compound

Procedure

Using the procedure described in Preparation 3, but replacing 3-methyl-6-acetylbenzoxazolin-3-one by 4-methyl-7-acetyl-2,3-dihydro-4H-1,4-benzothiazin-3-one and propionaldehyde by benzaldehyde, the product of the title is obtained.

Workup

  1. customdescribed in Preparation 3
  2. customthe product of the title is obtained

Sources & evidence

ORD record
ord-b4fb8ba0d7114ef1b0647d78890e9cdd
Source dataset
uspto-grants-1993_01
Patent number
US05179091

Reaction notes

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