HCID 53839528, compound → HCID 19801609, compound

Participants

Reaction Steps

A solution of ethyl N-[3-[3-(diethoxyphosphinyl)1-propenyl]phenyl]glycinate (Example 2a) in ethanol (75 ml) is treated with 10% palladium on carbon (0.25 g) and shaken on a Parr apparatus under a hydrogen atmosphere (50 pounds per square inch (psi)). After filtration, the filtrate is evaporated and the residue purified over silica gel (ethyl acetate as eluant) to give 1.24 g of a clear oil.

Provenance & Evidence