HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → N-[[2-(Phosphonomethyl)phenyl]methyl]glycine, hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 19801611 | HCID 19801611 | — |
| Product | N-[[2-(Phosphonomethyl)phenyl]methyl]glycine, hydrochloride | HCID 85635052 | — |
Reaction Steps
A solution of methyl N-[[2[(diethoxyphosphinyl)methyl]phenyl]methyl]glycinate (Example 1) (0.5 g, 1.5 mmol) in 6N hydrochloric acid solution (10 ml) is stirred at reflux in an oil bath for 18 hours. The water is removed in vacuo to give 0.4 g of a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05179085 |
| Source dataset | uspto-grants-1993_01 |
| ORD ID | ord-3cbc00c8eb004dacb065bb8bafcc3c18 |
| Source note | uspto-grants-1993_01 |