HRID1646179

反应详情

EQUATION

反应方程式

HRID 1646179 的结构方程式

PROCEDURE

实验过程

A solution of methyl N-[[2[(diethoxyphosphinyl)methyl]phenyl]methyl]glycinate (Example 1) (0.5 g, 1.5 mmol) in 6N hydrochloric acid solution (10 ml) is stirred at reflux in an oil bath for 18 hours. The water is removed in vacuo to give 0.4 g of a white solid.

WORKUP

后处理

  1. temperatureat reflux in an oil bath for 18 hours
  2. customThe water is removed in vacuo