HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15171982, compound → HCID 15171984, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15171982 | HCID 15171982 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Ammonia | HCID 222 | — |
| Product | HCID 15171984 | HCID 15171984 | — |
Reaction Steps
A solution of diethyl[[3-(cyanomethyl)phenyl]methyl]phosphonate in methanolic ammonia is reduced under a hydrogen atmosphere (50 psi) with Raney nickel as catalyst. The solvent is evaporated to give an oil (4.1 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05179085 |
| Source dataset | uspto-grants-1993_01 |
| ORD ID | ord-cb430c6a2dfa44249f11c8a14a2eb05f |
| Source note | uspto-grants-1993_01 |