HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → HCID 15106923, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Decane | HCID 15600 | — |
| Reactant | 5-chlorocarbonyl-5,10-dihydro-11H-dibenzo[b,e][1,4]diazepin-11-one | HCID 13276745 | — |
| Product | HCID 15106923 | HCID 15106923 | 30% |
Reaction Steps
Prepared analogously to Example 14 from 1.40 g (5.1 mmoles) of 5-(chlorocarbonyl)-5,10-dihydro-11H-dibenzo [b,e][1,4]diazepin-11-one, 0.78 g (5.12 mmoles) of 10-methyl-4,10- diazatricyclo[5.2.1.0z.° ]decane, 0.7 ml (5.1 mmoles) of triethylamine and 60 ml of acetonitrile in a yield of 30% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05179090 |
| Source dataset | uspto-grants-1993_01 |
| ORD ID | ord-03f32d49d3c64d05a8dcddcc1545bd07 |
| Source note | uspto-grants-1993_01 |