HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl bromoacetate → HCID 10019034, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl bromoacetate | HCID 7748 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 10421619 | HCID 10421619 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 10019034 | HCID 10019034 | — |
Reaction Steps
To a solution of 11-amino-4,5-dihydro-1H-pyrazolo[3,4-a]acridine (10 g) in dry DMF (300 ml) was added NaH (60%)(2.12 g) slowly. The reaction was stirred at room temperature for two hours, ethyl bromoacetate (6.0 ml) was added and the reaction was stirred for one hour.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05179100 |
| Source dataset | uspto-grants-1993_01 |
| ORD ID | ord-652a0e3d97f5479c8d3f709e5d1cefa0 |
| Source note | uspto-grants-1993_01 |