HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Ethylhexanoyl chloride → Methyl 4-[5-(2-ethylhexanamido)indol-3-ylmethyl]-3methoxybenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Ethylhexanoyl chloride | HCID 79103 | — |
| Reactant | Methyl 4-(5-aminoindol-3-ylmethyl)-3-methoxybenzoate | HCID 23365920 | — |
| Product | Methyl 4-[5-(2-ethylhexanamido)indol-3-ylmethyl]-3methoxybenzoate | HCID 23365894 | 6% |
Reaction Steps
Using a similar procedure to that described in Example 1, but starting from 2-ethylhexanoyl chloride and (A), there was obtained the title compound in 6% yield; partial NMR: 0.84 (m,6 H, 2×CH3), 1.24 [m,6 H, (CH2)3 ], 2.24 (m,1 H, CHCON), 10.78 (d,1 H, NH).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05179112 |
| Source dataset | uspto-grants-1993_01 |
| ORD ID | ord-a2f54a20ccfb4c569ed0201eca093108 |
| Source note | uspto-grants-1993_01 |