HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-methyl-2-pyrrolidone → HCID 15158253, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Reactant | 4,6-Dichloropyrimidine | HCID 70943 | — |
| Reactant | 9-Aminocarbazole | HCID 276207 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 15158253 | HCID 15158253 | — |
Reaction Conditions
| Temperature | 100 °C |
|---|
Reaction Steps
To 150 ml of 1-methyl-2-pyrrolidinone was added 10.0 g of 9H-carbazol-9-amine, and 8.2 g of 4,6-dichloropyrimidine, and the mixture was heated to 100° C. and stirred for eleven hours. The mixture was then poured into water and extracted with toluene. The organic layer was washed with water and dried (sat. NaCl, anhydrous MgSO4).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05179204 |
| Source dataset | uspto-grants-1993_01 |
| ORD ID | ord-c3daedecd5fa4c1fbddc27c3859b9f1c |
| Source note | uspto-grants-1993_01 |