Phenylhydrazine → 1H-Indole, 3-butyl-2-methyl-

HRID 1646409Notes

Reaction equation

[C:1]1([NH:7]N)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:9][C:10](=O)[CH2:11][CH2:12][CH2:13][CH2:14][CH3:15]>>[CH3:9][C:10]1[NH:7][C:1]2[C:6]([C:11]=1[CH2:12][CH2:13][CH2:14][CH3:15])=[CH:5][CH:4]=[CH:3][CH:2]=2

Participants

Reactant 2

HCID 7516Phenylhydrazine

HCID 80512-Heptanone

Product 1

HCID 122748871H-Indole, 3-butyl-2-methyl-Yield 38%

Procedure

Phenylhydrazine was reacted with heptan-2-one in the same way as in Example 2. 2-Methyl-3-butylindole was formed in a yield of 38%.

Sources & evidence

ORD record: ord-ef87286d635444828eb8e62ebacad32f
Source dataset: uspto-grants-1993_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05179211

Reaction notes

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