HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → HCID 19746782, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | HCID 19746749 | HCID 19746749 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 19746782 | HCID 19746782 | 44% |
Reaction Steps
Bromination of 2,4-bis(p-chlorophenyl)-5-cyanopyrrole is accomplished by treatment with 1 equivalent of bromine in acetic acid in the presence of anhydrous sodium acetate yields the desired product (0.47 g, yellow solid, 44% yield, mp 98°-100° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05180734 |
| Source dataset | uspto-grants-1993_01 |
| ORD ID | ord-d3cf31a90c7d484195e9a1dc2e3c1840 |
| Source note | uspto-grants-1993_01 |