HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methane → HCID 19801168, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methane | HCID 297 | — |
| Reactant | HCID 19801174 | HCID 19801174 | — |
| Catalyst | Rhodium | HCID 23948 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19801168 | HCID 19801168 | 94.6% |
Reaction Steps
1.63 g of 4-(2-propenyl)-1-indanone is dissolved in 300 ml of anhydrous ethanol and 400 mg of rhodium at 5% on active charcoal and hydrogenated at ambient temperature and ambient pressure for 3/4 hour. After filtering on celite, the filtrate is washed with ethanol and evaporated to dryness, and 1.56 g of expected product is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05180741 |
| Source dataset | uspto-grants-1993_01 |
| ORD ID | ord-c0c78295377a4533940621875516aa4f |
| Source note | uspto-grants-1993_01 |