Hydrogen Peroxide → HCID 86746509, compound

Participants

Reaction Steps

To a stirring solution of 0.7 g (1.5 mmol) of 8-chlorodibenzo[b,f][1,4]thiazepine-10(11H)-carboxylic acid, 2-[1-oxo-3-[(2-thienylacetyl)amino]propyl]hydrazide (37), prepared in the manner described above in Example 37, in 5 mL of HOAc is added 0.13 mL (1.5 mmol) of 30% H2O2. After stirring for 1 hour, the reaction mixture is lyophilized to obtain the product.

Provenance & Evidence