Hydrochloric Acid → HCID 131717721, compound

HRID 1646915Notes

Reaction equation

HRID 1646915 reaction equation
[NH2:1][C@H:2]([C:6]([NH:8][C@H:9]([C:14]([NH:16][C@@H:17]([C:26]([OH:28])=[O:27])[CH2:18][C:19]1[CH:24]=[CH:23][C:22]([OH:25])=[CH:21][CH:20]=1)=[O:15])[CH2:10][C:11](=[O:13])[OH:12])=[O:7])[C@@H:3]([CH3:5])[OH:4].[ClH:29]>O>[NH2:1][C@H:2]([C:6]([NH:8][C@H:9]([C:14]([NH:16][C@@H:17]([C:26]([OH:28])=[O:27])[CH2:18][C:19]1[CH:24]=[CH:23][C:22]([OH:25])=[CH:21][CH:20]=1)=[O:15])[CH2:10][C:11](=[O:12])[OH:13])=[O:7])[C@@H:3]([CH3:5])[OH:4].[ClH:29]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 58753139HCID 58753139, compound

Product 1

HCID 131717721HCID 131717721, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

H-Thr-Asp-D-Tyr-OH is dissolved in 5 volumes of water, and the solution is added with an equivalent amount of 1N HCl. By freeze-drying or diluting with acetone the solution, the hydrochloride is obtained as a very water soluble powder.

Workup

  1. customBy freeze-drying
  2. additiondiluting with acetone the solution

Sources & evidence

ORD record
ord-c6c2ee01c8704396b47b8a2d9dd62611
Source dataset
uspto-grants-1993_01
Patent number
US05182265

Reaction notes

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