Potassium Carbonate → HCID 19800290, compound

HRID 1646971Notes

Reaction equation

[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]#[C:9][Si](C)(C)C)=[CH:4][C:3]=1[O:14][CH3:15].C(=O)([O-])[O-].[K+].[K+]>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]#[CH:9])=[CH:4][C:3]=1[O:14][CH3:15]

Participants

Reactant 2

HCID 11430Potassium Carbonate

HCID 198003224-Chloro-3-methoxyphenylethynyl-trimethylsilane

Product 1

HCID 19800290HCID 19800290, compoundYield 93.2%

Procedure

Using the procedure of Step C of Preparation 14, 8 g of the product of Step A and 0.46 g of potassium carbonate were reacted to obtain 5.2 g of the expected product.

Workup

customwere reacted

Sources & evidence

ORD record: ord-5282f9c1e43649d5ab69722ce4cfabc4
Source dataset: uspto-grants-1993_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05182295

Reaction notes

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