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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1646995Generated: October 31, 2026

2-Aminobenzaldehyde → HCID 10005431, compound

https://huagongshe.com/reaction/1646995

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-AminobenzaldehydeHCID 68255—
ReactantHCID 14771497HCID 14771497—
SolventDiethyl EtherHCID 3283—
ProductHCID 10005431HCID 10005431—

Reaction Conditions

Temperature185 °C

Reaction Steps

In a sealed tube a mixture of 0.02 mol of 2-aminobenzaldehyde and 0.02 mol of 1-(4-tosyloxybenzenesulphonyl)-3-methyl-butan-2-one was heated at 185° C. for 2 hours. The mixture was then taken up in dry ethyl ether and filtered. M.P. of the hydrochloride: about 90° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05182291
Source datasetuspto-grants-1993_01
ORD IDord-0b770be041e14966b9d2dceafcdcbde7
Source noteuspto-grants-1993_01