Allylamine → HCID 19926920, compound

HRID 1647286Notes

Reaction equation

[C:1]([C:4]1[C:5](=[O:22])[NH:6][C:7]2[C:12]([C:13]=1C)=[C:11](OS(O)(=O)=O)[C:10]([CH3:20])=[CH:9][C:8]=2[Cl:21])(=[O:3])[CH3:2].[CH2:23]([NH2:26])[CH:24]=[CH2:25]>>[C:1]([C:4]1[C:5](=[O:22])[NH:6][C:7]2[C:12]([C:13]=1[NH:26][CH2:23][CH:24]=[CH2:25])=[CH:11][C:10]([CH3:20])=[CH:9][C:8]=2[Cl:21])(=[O:3])[CH3:2]

Participants

Reactant 2

HCID 7853Allylamine

HCID 19926935HCID 19926935, compound

Product 1

HCID 19926920HCID 19926920, compoundYield 82%

Procedure

3-Acetyl-8-chloro-6-methyl-4 -methylsulfoxy -2-quinolinone (2.97 g, 0.01 mol) and allylamine (0.57g, 0.01 mol) were used, but the reaction was carried out as the above process of example 37 to obtain the desired product (2.38g, yield: 82%).

Sources & evidence

ORD record: ord-44e33a71d2c741c8b74bccb1e90886d9
Source dataset: uspto-grants-1995_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05430153

Reaction notes

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