HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 22068494, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 76412589 | HCID 76412589 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22068494 | HCID 22068494 | — |
Reaction Steps
To 2.35 g of product from Example 1 in 10 ml of methylene chloride is added 2.8 ml of trifluoroacetic acid. The reaction is heated at 80°-90° C. for 41/2 hours and then concentrated in vacuo to give 3.6 g of the desired product as tris-trifluoroacetic acid salt.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05430150 |
| Source dataset | uspto-grants-1995_07 |
| ORD ID | ord-43256b58bc5b4173b025d1b611230fc9 |
| Source note | uspto-grants-1995_07 |