Trifluoroacetic acid → HCID 22068505, compound

HRID 1647339Notes

Reaction equation

HRID 1647339 reaction equation
CC(OC(=O)[NH:7][CH:8]([C:13]([NH:15][CH2:16][C:17]1[CH:18]=[N:19][CH:20]=[CH:21][CH:22]=1)=[O:14])[CH:9]([CH3:12])[CH2:10][CH3:11])(C)C.[F:24][C:25]([F:30])([F:29])[C:26]([OH:28])=[O:27]>>[F:24][C:25]([F:30])([F:29])[C:26]([OH:28])=[O:27].[NH2:7][CH:8]([CH:9]([CH3:12])[CH2:10][CH3:11])[C:13]([NH:15][CH2:16][C:17]1[CH:18]=[N:19][CH:20]=[CH:21][CH:22]=1)=[O:14]

Participants

3

Reactant 2

HCID 6422Trifluoroacetic acidHCID 67781312HCID 67781312, compound

Product 1

HCID 22068505HCID 22068505, compoundYield 172.5%

Procedure

The title compound is prepared by the procedure of Example 2, using 2.0 g of product from Example 3 and 3.55 g of trifluoroacetic acid to give 3.6 g of the desired product as a tacky oil.

Workup

  1. customThe title compound is prepared by the procedure of Example 2

Sources & evidence

ORD record
ord-8a5e5e844db44ca9a2ea9429794960fd
Source dataset
uspto-grants-1995_07
Patent number
US05430150

Reaction notes

Loading…