HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorotrimethylsilane → Leucyl-leucine-methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorotrimethylsilane | HCID 6397 | — |
| Reactant | L-leucine L-leucine | HCID 22842050 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Leucyl-leucine-methyl ester | HCID 7016877 | — |
Reaction Steps
To 0.50 g of L-leucine-L-leucine, under argon, is added, via a syringe, 10 ml of methyl alcohol and 0.610 ml of trimethylsilyl chloride. The reaction is stirred overnight at room temperature. The mixture is concentrated in vacuo to give 0.554 g of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05430150 |
| Source dataset | uspto-grants-1995_07 |
| ORD ID | ord-ff76d6afcc7f43d2a52e1c24cc33943a |
| Source note | uspto-grants-1995_07 |