HRID1647346

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID6422

未命名化合物

2 次

结构：CCC(C)C(NC(=O)OC(C)(C)C)C(=O)NCc1nc2ccccc2[nH]1

HCID67747066

未命名化合物

PRODUCTS

生成物

结构：CCC(C)C(N)C(=O)NCc1nc2ccccc2[nH]1.O=C(O)C(F)(F)F.O=C(O)C(F)(F)F.O=C(O)C(F)(F)F

HCID22068508

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

The title compound is prepared by the procedure of Example 2 using 0.588 g of product from Example 11 in 6 ml of methylene chloride and 1.3 g of trifluoroacetic acid (TFA). The resulting desired intermediate is used as is in the next reaction. The 1HNMR indicates the correct product with associated TFA molecules.

WORKUP

后处理

customas is in the next reaction