HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 41473673, compound → 1H-Benzimidazole-2-methanamine,alpha-methyl-,(R)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 41473673 | HCID 41473673 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 1H-Benzimidazole-2-methanamine,alpha-methyl-,(R)- | HCID 693233 | 82.2% |
Reaction Steps
The title compound is prepared by the procedure of Example 15, in a Parr apparatus, using 1.07 g of product from Example 44, 90 ml of methyl alcohol and 2.45 g of 10% palladium on carbon to give 0.48 g of the desired product after recrystallization from carbon tetrachloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05430150 |
| Source dataset | uspto-grants-1995_07 |
| ORD ID | ord-b4e99cbdce28429d8e125314d9669e96 |
| Source note | uspto-grants-1995_07 |