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HRID1647365

反应详情

EQUATION

反应方程式

HRID 1647365 的结构方程式

REACTANTS

反应物

4
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：O
HCID962

Water

H2O

结构：CCOCC
HCID3283

Diethyl Ether

C4H10O

结构：COC(=O)[C@H](CO)NC(=O)C(Cc1ccccc1)N1C(=O)c2ccccc2C1=O
HCID67799768

未命名化合物

PRODUCTS

生成物

1
结构：C=CCCC(N)C(=O)OC
HCID15356347

Methyl 2-aminohex-5-enoate

C7H13NO2

PROCEDURE

实验过程

Dissolve N-(phenylmethylene)-2-(3-butenyl)glycine methyl ester (25g) in ethyl ether (400mL) and stir with 1N hydrochloric acid (150mL) and water (150mL). Place under an argon atmosphere and stir for 2 hours. Separate the aqueous phase and adjust to pH 9, extract into chloroform, dry and evaporate the solvent in vacuo to give the title compound as a light oil (4.5g).

WORKUP

后处理

  1. customSeparate the aqueous phase
  2. extractionextract into chloroform
  3. customdry
  4. customevaporate the solvent in vacuo