HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Aminobenzyl alcohol → HCID 178450496, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Aminobenzyl alcohol | HCID 69331 | — |
| Reactant | Ethyl 2-butyryl-3-ethoxyacrylate | HCID 3359484 | — |
| Product | HCID 178450496 | HCID 178450496 | — |
Reaction Steps
4-Aminobenzylalcohol (25 g) and ethyl 2-butyryl-3-ethoxyacrylate (61 g) were heated together on a rotary evaporator (bath temp 100°) for 30 minutes. Ethyl 2-butyryl-3-(4-(hydroxymethyl)phenylamino)acrylate (49.5 g, 84%) crystallized on standing, was filtered off, washed with a little petroleum ether and vacuum dried, m.p. 44°-6°
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05432182 |
| Source dataset | uspto-grants-1995_07 |
| ORD ID | ord-cbce1098426f4f74b92c14e8bfb4ddba |
| Source note | uspto-grants-1995_07 |