HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1647493Generated: November 3, 2026
Methanesulfonic Acid → HCID 86748781, compound
https://huagongshe.com/reaction/1647493
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | HCID 9887258 | HCID 9887258 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 86748781 | HCID 86748781 | — |
Reaction Steps
3-Butyryl-4-(2-methylphenylamino)-8-(2-hydroxyethoxy)quinoline (60 g) was suspended in ethyl acetate (400 ml), warmed to 50° C., and methanesulphonic acid (16.3 g) added with vigorous stirring. The desired salt crystallised on cooling, and was filtered off and washed with ethyl acetate; yield 50.1 g, m.p. 83°-85° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05432182 |
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| Source dataset | uspto-grants-1995_07 |
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| ORD ID | ord-7fa8c75cac4a4ad5a638e060d201174c |
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| Source note | uspto-grants-1995_07 |
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