HCID 67283741, compound → HCID 178421249, compound

Participants

Reaction Steps

To a solution of 0.10 g of 3β-(3-aminopropoxy)-17β-(3-furyl)-5β-androstan-14β-ol (I-ab) in 7 ml of absolute ethanol 0.060 g of 3,5-dimethyl-1-pyrazolylformamidinium nitrate were added and the mixture was kept at reflux temperature for 24 hrs; the ethanol was concentrated under reduced pressure and 0.090 g of the title compound (I-am) crystallized as a white solid.

Provenance & Evidence