Hydrochloric Acid → HCID 67806122, compound

HRID 1647874Notes

Reaction equation

HRID 1647874 reaction equation
[ClH:1].[CH3:2][O:3][C:4]([CH2:6][CH2:7][NH:8][C:9](=[O:27])[C:10]1[CH:15]=[CH:14][C:13]([NH:16][CH2:17][CH2:18][CH2:19]N2CCSCC2)=[C:12]([NH2:26])[CH:11]=1)=[O:5].Cl>C(Cl)Cl.CO>[ClH:1].[CH3:2][O:3][C:4]([CH2:6][CH2:7][NH:8][C:9](=[O:27])[C:10]1[CH:15]=[CH:14][C:13]([NH:16][CH2:17][CH2:18][CH2:19][C:4]([O:3][CH3:2])=[O:5])=[C:12]([NH2:26])[CH:11]=1)=[O:5]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 67806829HCID 67806829, compound

Product 1

HCID 67806122HCID 67806122, compound

Reagents, catalysts & solvents 1

HCID 21226129Dichloromethane methanolSolvent

Procedure

The same procedure is used as in (2) with the addition of ethereal hydrochloric acid. Rf value: 0.65 (silica gel; methylene chloride/Methanol=9:1)

Sources & evidence

ORD record
ord-d9f1bbae91af4ca28835d61c1f5df44a
Source dataset
uspto-grants-1995_07
Patent number
US05434150

Reaction notes

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