HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 19921428, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 19921473 | HCID 19921473 | — |
| Reactant | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 19921428 | HCID 19921428 | — |
Reaction Steps
The same procedure is used as in (1) using triethylamine as auxiliary base. A 3:1 mixture of tetrahydrofuran and methylene chloride is used as solvent. Rf value: 0.68 (silica gel; methylene chloride/methanol=37:3)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05434150 |
| Source dataset | uspto-grants-1995_07 |
| ORD ID | ord-c3bad4d3e9644085bf3bcd775d26e2ed |
| Source note | uspto-grants-1995_07 |