Diethylphosphorylcyanide → HCID 178477256, compound

HRID 1647899Notes

Reaction equation

HRID 1647899 reaction equation
[C:1]([C:4]1[CH:9]=[CH:8][C:7]([C:10]2[N:14]([CH2:15][CH2:16][CH2:17][CH2:18][C:19]3[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=3)[C:13]3[CH:25]=[CH:26][C:27]([C:29]([NH:31][CH2:32][CH2:33][C:34]([O:36][CH3:37])=[O:35])=[O:30])=[CH:28][C:12]=3[N:11]=2)=[CH:6][CH:5]=1)(=[NH:3])[NH2:2].[CH2:38]([P:40](C#N)([CH2:42][CH3:43])=[O:41])[CH3:39]>CN(C)C=O>[CH2:38]([P:40]([NH:3][C:1]([C:4]1[CH:5]=[CH:6][C:7]([C:10]2[N:14]([CH2:15][CH2:16][CH2:17][CH2:18][C:19]3[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=3)[C:13]3[CH:25]=[CH:26][C:27]([C:29]([NH:31][CH2:32][CH2:33][C:34]([O:36][CH3:37])=[O:35])=[O:30])=[CH:28][C:12]=3[N:11]=2)=[CH:8][CH:9]=1)=[NH:2])([CH2:42][CH3:43])=[O:41])[CH3:39]

Participants

4

Reactant 2

HCID 13586794DiethylphosphorylcyanideHCID 19921410HCID 19921410, compound

Product 1

HCID 178477256HCID 178477256, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

Prepared by reacting 2-(4-amidino-phenyl)-5-[(2-methoxycarbonyl-ethyl)-aminocarbonyl]-1-(4-phenyl-butyl)-benzimidazole with diethylphosphorylcyanide in dimethylformamide.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-f6a009954b56420c8dd30cef3faab226
Source dataset
uspto-grants-1995_07
Patent number
US05434150

Reaction notes

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