HRID1648171

反应详情

EQUATION

反应方程式

HRID 1648171 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

In a 10 l autoclave, 92 g of glycerol, 24 g of potassium hydroxide, 6,970 g of propylene oxide and 1,100 g of butylene oxide were fed and reacted together at 110° C. for 15 hours. After the reaction has been completed, the mixture was neutralized and desalted to obtain 8,100 g of a trifunctional propylene oxide-butylene oxide random copolymer. Its molecular weight was 8,145 (calculated from its hydroxyl number).

WORKUP

后处理

  1. customreacted together at 110° C. for 15 hours