HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Xylene → HCID 15376513, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Xylene | HCID 7237 | — |
| Reactant | 2,2-Dimethyl-5-phenyl-2H,4H-1,3-dioxin-4-one | HCID 13157033 | — |
| Reactant | HCID 15405502 | HCID 15405502 | — |
| Product | HCID 15376513 | HCID 15376513 | — |
Reaction Steps
Xylene (2 ml) was added to a mixture of 5-phenyl-2,2-dimethyl-2H,4H-1,3-dioxin-4-one (0.82 g) and N-methylene-1-methyl-1-phenylethylamine (0.59 g), and the resulting mixture was heated at reflux for 20 minutes for reaction. The reaction mixture was purified by silica gel chromatography to obtain the captioned compound (0.9 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05436224 |
| Source dataset | uspto-grants-1995_07 |
| ORD ID | ord-cba4ffcbabdc4382a3078b687bc90027 |
| Source note | uspto-grants-1995_07 |