HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Pyridinecarboxaldehyde → HCID 135491709, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Pyridinecarboxaldehyde | HCID 10371 | — |
| Reactant | 2-Methyl-4(3H)-quinazolinone | HCID 135400457 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 135491709 | HCID 135491709 | — |
Reaction Steps
A mixture of 2-methylquinazolin-4-one (6.1 g) and 3-pyridinecarbaldehyde (4.1 g) in acetic acid (80 mL) was heated to reflux for 20 hours. After cooling to room temperature, the precipitate was collected by filtration, washed with methanol and dried to obtain the title compound as an acetic acid salt (10.5 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05436233 |
| Source dataset | uspto-grants-1995_07 |
| ORD ID | ord-6fa5af23a148440ebe29a6d8f8488670 |
| Source note | uspto-grants-1995_07 |