HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → HCID 10082813, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | 1-Tetralone | HCID 10724 | — |
| Solvent | Toluene water | HCID 22272177 | — |
| Product | HCID 10082813 | HCID 10082813 | — |
Reaction Steps
A mixture containing 171 mmol of-tetralone, 181 mmol of benzylamine and 100 mg of p-toluenesulfonic acid is brought to reflux with azeotropic distillation of the water/toluene mixture. After 2 hours of distillation, the medium is cooled and filtered. The expected product is obtained in the form of an oil after evaporation of the solvent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05436261 |
| Source dataset | uspto-grants-1995_07 |
| ORD ID | ord-2f1bd10ecf5945bcbcc3ed5f62cbec8b |
| Source note | uspto-grants-1995_07 |