HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 19920015, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 19920017 | HCID 19920017 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 19920015 | HCID 19920015 | — |
Reaction Steps
The product prepared in step (e) above is added, with stirring, to 5 to 10 times excess of ammonia. The mixture is stirred at room temperature for 3 hours. An excess of ether is then added and the precipitate is filtered off. The ether is removed in vacuo and the resulting oil is used directly to prepare the hydrochloride salt.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05436273 |
| Source dataset | uspto-grants-1995_07 |
| ORD ID | ord-959750ab866e418085985bdf8984c4d6 |
| Source note | uspto-grants-1995_07 |