Hydrochloric Acid → HCID 19919732, compound

Participants

Reaction Steps

A solution of 10.55 g of 2-amino-1-(3,5-dimethyl-4-methoxymethoxyphenyl)ethanol [prepared as described in step (b), above] in 200 ml of a 4N solution of hydrogen chloride in dioxane was stirred at room temperature for 18 hours. The solvent was then removed by distillation under reduced pressure, to give 10.45 g of the title compound, melting at between 170° C. and 172° C.

Provenance & Evidence