HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → HCID 86739105, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | Chlorine | HCID 24526 | — |
| Reactant | Sulfuryl chloride | HCID 24648 | — |
| Reactant | HCID 20481811 | HCID 20481811 | — |
| Reactant | HCID 178484910 | HCID 178484910 | — |
| Reactant | HCID 178484923 | HCID 178484923 | — |
| Product | HCID 86739105 | HCID 86739105 | 14% |
Reaction Steps
Following the procedure for Example 2, but substituting N,N'-dithiobis[N-pheylmethanesulfonamide] for N,N'-dithiobis-[N-isopropyl-p-toluenesulfonamide], chlorine for sulfuryl chloride, and N-methyl-N'-2,4-xylylformamidine for N-methyl-N'-(4-chloro-o-tolyl) formamidine, the product is prepared. The product is recrytallized from ethyl acetate to give 2.0 g. (14% yield) of N-[[[N-2,4-xylylformimidoyl]methylamino]thio]-N-phenylmethanesulfonamide as white crystals, mp. 120°-121.5°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04413013 |
| Source dataset | uspto-grants-1983_11 |
| ORD ID | ord-07d2941ceb6a4c18abc986f46e81cbbd |
| Source note | uspto-grants-1983_11 |