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HRID1648795

反应详情

EQUATION

反应方程式

HRID 1648795 的结构方程式

REACTANTS

反应物

6
结构：CCOC(C)=O
HCID8857

Ethyl acetate

C4H8O2

结构：ClCl
HCID24526

Chlorine

Cl2

结构：O=S(=O)(Cl)Cl
HCID24648

Sulfuryl chloride

Cl2O2S

结构：Cc1ccc(S(=O)(=O)N(SSN(C(C)C)S(=O)(=O)c2ccc(C)cc2)C(C)C)cc1
HCID20481811

未命名化合物

结构：CNC=Nc1ccc(C)cc1C
HCID178484910

未命名化合物

结构：CNC=Nc1cc(Cl)ccc1C
HCID178484923

未命名化合物

PRODUCTS

生成物

1
结构：Cc1ccc(N=CCNSN(c2ccccc2)S(C)(=O)=O)c(C)c1
HCID86739105

未命名化合物

收率 14%

PROCEDURE

实验过程

Following the procedure for Example 2, but substituting N,N'-dithiobis[N-pheylmethanesulfonamide] for N,N'-dithiobis-[N-isopropyl-p-toluenesulfonamide], chlorine for sulfuryl chloride, and N-methyl-N'-2,4-xylylformamidine for N-methyl-N'-(4-chloro-o-tolyl) formamidine, the product is prepared. The product is recrytallized from ethyl acetate to give 2.0 g. (14% yield) of N-[[[N-2,4-xylylformimidoyl]methylamino]thio]-N-phenylmethanesulfonamide as white crystals, mp. 120°-121.5°.

WORKUP

后处理

  1. customthe product is prepared
  2. customto give 2.0 g