HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2,6,6-Tetramethyl-4-piperidone → 5,5,7,7-Tetramethyl-1-oxa-6-azaspiro[2.5]octane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2,6,6-Tetramethyl-4-piperidone | HCID 13220 | — |
| Reactant | HCID 178418582 | HCID 178418582 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 5,5,7,7-Tetramethyl-1-oxa-6-azaspiro[2.5]octane | HCID 20671094 | — |
Reaction Steps
44.55 g (0.825 mole) of CH3ONa were added to the mixture, under stirring, and, in half an hour, a solution of 77.5 g (0.5 mole) of triacetonamine dissolved in 50 cc of CH3CN was gradually added.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04413075 |
| Source dataset | uspto-grants-1983_11 |
| ORD ID | ord-5e04cf749018489f93e60a10a7559722 |
| Source note | uspto-grants-1983_11 |