HuagongsheHuagongshe Chemistry Print Report · For research reference only
4H-1,2,4-Triazol-4-amine, 3,5-bis(2-chlorophenyl)- → Bekrxdrmajampz-uhfffaoysa-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4H-1,2,4-Triazol-4-amine, 3,5-bis(2-chlorophenyl)- | HCID 826306 | — |
| Reactant | Sodium Nitrite | HCID 23668193 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Water | HCID 962 | — |
| Product | Bekrxdrmajampz-uhfffaoysa- | HCID 11000759 | 52.3% |
Reaction Steps
The product of stage (a) (19.5 g) was dissolved in glacial acetic acid (100 ml) and was treated with sodium nitrite (4.4 g) in water (15 ml) at 10° C. The precipitated solid was filtered off, washed, dried and recrystallised from methanol to yield 9.7 g of desired product, mp 159°-160° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04414221 |
| Source dataset | uspto-grants-1983_11 |
| ORD ID | ord-b6f615d23d0a4bf48eee9775f236e28d |
| Source note | uspto-grants-1983_11 |