Triethylamine → Methylthiomethyl 2-Methyl-2-pentenoate

HRID 1648903Notes

Reaction equation

HRID 1648903 reaction equation
[CH3:1][C:2](=[CH:6][CH2:7][CH3:8])[C:3]([OH:5])=[O:4].[CH3:9][S:10][CH2:11]Cl.C(N(CC)CC)C>>[CH3:1][C:2](=[CH:6][CH2:7][CH3:8])[C:3]([O:5][CH2:9][S:10][CH3:11])=[O:4]

Participants

4

Reactant 3

HCID 8471TriethylamineHCID 16916Chloromethyl methyl sulfideHCID 184582-Methylpent-2-en-1-oic acid

Product 1

HCID 54484466Methylthiomethyl 2-Methyl-2-pentenoate

Procedure

This product was prepared according to the procedure described in Example 1, by reacting 2-methyl-2-pentenoic acid with chloromethyl methyl sulfide in the presence of one equivalent of triethylamine; b.p. 56°-57° C./2 mm Hg, n20 1.4861.

Workup

  1. customThis product was prepared

Sources & evidence

ORD record
ord-af6ea1e2151e498085c45ec404929c99
Source dataset
uspto-grants-1983_11
Patent number
US04414233

Reaction notes

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