HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 70532075, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | 4-Vinylpyridine | HCID 7502 | — |
| Reactant | Octahydropyrrolo(1,2-a)pyrazine | HCID 558578 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 70532075 | HCID 70532075 | — |
Reaction Steps
A solution of 12 g (0.095 mole) 1,4-diazabicyclo[4.3.0]-nonane, 10 ml of acetic acid and 12.5 ml of 4-vinylpyridine in 225 ml methanol was heated at reflux for 20 hours. The solvent was removed under vacuum and the residue distilled to yield 5.1 g of 2(4-pyridylethyl)pyrrolo[1,2-a]pyrazine; b.p. 126°-130/0.01 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04414389 |
| Source dataset | uspto-grants-1983_11 |
| ORD ID | ord-e82213dc57e44b46be0efe9df57f17d6 |
| Source note | uspto-grants-1983_11 |