Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 13260265 | HCID 13260265 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 20481482 | HCID 20481482 | — |
Reaction Steps
To a suspension of 5-(3-dimethylaminomethylimidazo[1,2-a]pyridine-2-yl)-8-methoxycarbostyril (1.5 g) in acetonitrile (20 ml) was added methyl iodide (1.5 ml) and the mixture was stirred at 40° C. for 1 hour. Crystals thus formed were collected by filtration and recrystallized from water to give 1.7 g of 5-(3-trimethylammoniomethylimidazo[1,2-a]pyridine-2-yl)-8-methoxycarbostyril iodide trihydrate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04414390 |
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| Source dataset | uspto-grants-1983_11 |
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| ORD ID | ord-c1b45834122b4ede8c4aeba3fc3ccd2b |
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| Source note | uspto-grants-1983_11 |
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