HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 53929801, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Ethanone, 1,1′-(4-amino-6-hydroxy-1,3-phenylene)bis- | HCID 20230855 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 53929801 | HCID 53929801 | — |
Reaction Steps
Treatment of the product of step (b) (1.5 g) with K2CO3 (1 equivalent) and allyl bromide (2 equivalents) in dimethylformamide (20 ml) at 70° C. for 21/2 hours followed by dilution with water at 70° C. afforded the sub-title product, as a pale yellow solid (83%) mp 131°-134°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04414416 |
| Source dataset | uspto-grants-1983_11 |
| ORD ID | ord-2987dc3d1c0e4b079a0d6c514c3ea034 |
| Source note | uspto-grants-1983_11 |