Butylamine → HCID 13138304, compound

Participants

Reaction Steps

2-Amino-4-chloro-6-(3,4-dichlorophenyl)-s-triazine (melting point 249° to 250° C.) (2.75 grams) and 2.0 grams of n-butylamine were heated to reflux with stirring for four hours in 25 milliliters of dioxane. The reaction solution was evaporated to dryness in vacuo, the residue was washed with water and then with methanol, and 2.51 grams of 2-amino-4-butylamino-6-(3,4-dichlorophenyl)-s-triazine was obtained. Melting point 176° to 179° C.

Provenance & Evidence