Acetic Anhydride → HCID 13057121, compound

HRID 1649104Notes

Reaction equation

HRID 1649104 reaction equation
[C:1]([O:4][CH2:5][CH2:6][O:7][CH2:8][N:9]1[CH:16]=[C:15]([F:17])[C:13](=[O:14])[NH:12][C:10]1=[O:11])(=[O:3])[CH3:2].[C:18](OC(=O)C)(=O)C>N1C=CC=CC=1>[C:1]([O:4][CH2:5][CH2:6][O:7][CH:8]([N:9]1[CH:16]=[C:15]([F:17])[C:13](=[O:14])[NH:12][C:10]1=[O:11])[CH3:18])(=[O:3])[CH3:2]

Participants

4

Reactant 2

HCID 7918Acetic AnhydrideHCID 4443484HCID 4443484, compound

Product 1

HCID 13057121HCID 13057121, compound

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

1-[1-(2-Hydroxyethoxy)ethyl]-5-fluorouracil (2 g) obtained in Example 2 was treated with acetic anhydride and pyridine as in Example 2 to give 2 g of 1-[1-(2-acetoxyethoxy)-ethyl]-5-fluorouracil.

Sources & evidence

ORD record
ord-1f86a3e040c74181b5726f13c70027b2
Source dataset
uspto-grants-1983_11
Patent number
US04415573

Reaction notes

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