HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Fluorouracil → HCID 15583560, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Fluorouracil | HCID 3385 | — |
| Reactant | 3,4-Diacetoxybenzaldehyde | HCID 1517488 | — |
| Reactant | HCID 20480611 | HCID 20480611 | — |
| Reactant | HCID 68585259 | HCID 68585259 | — |
| Solvent | Ethylene Glycol | HCID 174 | — |
| Product | HCID 15583560 | HCID 15583560 | — |
Reaction Steps
Bis(trimethylsilyl)-5-fluorouracil prepared from 5-fluorouracil (10 g) , and 2-(3,4-diacetoxyphenyl)-1,3-dioxolan (26.6 g) prepared from 3,4-diacetoxybenzaldehyde and ethyleneglycol were treated as in Example 10 and the product was acetylated to give 7.4 g of crystalline 1-[α-(2-acetoxyethoxy)-3,4-diacetoxybenzyl]-5-fluorouracil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04415573 |
| Source dataset | uspto-grants-1983_11 |
| ORD ID | ord-74ab5c98af824f55a0df67aaccd15aae |
| Source note | uspto-grants-1983_11 |