Sodium Bicarbonate → HCID 23668221, compound

Participants

Reaction Steps

To a solution of 6.79 g (16.7 mmol) of 4-(4,4-dimethyl-4-sila-hexadecylamino)benzoic acid in 10 ml of ethanol is added an aqueous solution of 1.5 g (17.8 mmol) of sodium bicarbonate (in about 50 ml of water). The mixture is heated to 60° and the resultant clear solution evaporated, under vacuum, to obtain the title product as a white crystalline solid, m.p. above 300°.

Provenance & Evidence